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研究生: 蕭仲良
Chung-Liang Hsiao
論文名稱: 積層製造17-4 PH不鏽鋼之製程參數探討與高週疲勞性質研究
Study on the process parameters and high cycle fatigue properties of 17-4 PH stainless steel fabricated by additive manufacturing
指導教授: 黃俊仁
Jiun-Ren Hwang
口試委員:
學位類別: 碩士
Master
系所名稱: 工學院 - 機械工程學系
Department of Mechanical Engineering
論文出版年: 2022
畢業學年度: 110
語文別: 中文
論文頁數: 119
中文關鍵詞: 17-4 PH 不鏽鋼選擇性雷射熔融製造積層製造疲勞性質平均應力變動負荷振幅疲勞疲勞壽命預測模式
外文關鍵詞: 17-4 PH stainless steel, selective laser melting manufacturing, additive manufacturing, fatigue properties, mean stress, variable load amplitude fatigue, fatigue life prediction model
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  • 本研究以中等的雷射功率範圍 (120 W - 180 W) 對 17-4 PH 不鏽鋼進行選擇性雷射熔融積層製造。針對不同製程條件下之工件,比較其密度、硬度、表面粗糙度、金相與孔洞率。然後選取一組材料強度較高與孔洞率較少的參數組合,量測該工件之拉伸、固定負荷振幅疲勞及變動負荷振幅疲勞性質,並探討其疲勞壽命預測模式。
    研究結果顯示,在密度、硬度、表面粗糙度、孔洞率方面,當列印能量密度越高時,材料會呈現較高的密度值,與較高的硬度值。同時還有較低的表面粗糙度,與較少的孔洞率。列印參數組合為雷射功率 140 W、掃描速率 800 mm/s、掃描間距 80 μm、層厚 30 μm 之試件具有較高材料強度與較少孔洞率。本研究的選擇性雷射熔融積層製造工件的疲勞 S-N 曲線雖然小於鍛造試件,但是大於採用其他雷射功率 (250 W、220 W、48 W) 列印的工件。在固定負荷振幅疲勞方面,平均應力之修正以採用 Soderberg 方程式為最佳。在變動負荷振幅疲勞方面,不論是傳動軸歷程或支架歷程,Soderberg 修正式及 Goodman 修正式皆適用於預測 17-4 PH 不鏽鋼積層製造工件之疲勞壽命。


    In this study, selective laser melting (SLM) manufacturing was performed on 17-4 PH stainless steel in a moderate laser power range (120 W - 180 W). The density, hardness, surface roughness, metallography and porosity of the workpiece under different processing conditions were compared. Then a combination of the process parameters is selected, which has higher strength and less porosity. The properties of tensile, constant load amplitude fatigue and variable load amplitude fatigue were measured, and the fatigue life prediction model was discussed.
    The results show that the higher the printing energy density is, the higher the density and hardness will be. At the same time, it also has lower surface roughness and less porosity. The test sheet with laser power 140 W, scanning speed 800 mm/s, hatching spacing 80 μm, and layer thickness 30 μm has higher strength and less hole ratio. The S-N curve of the specimens in this study is lower than that of the wrought specimen, but it is higher than the curves printed by SLM with other laser powers (250 W, 220 W, 48 W). The Soderberg equation is the best method to correct the mean stress effect under constant amplitude fatigue loading. Soderberg's mean stress modification or Goodman's mean stress modification methods are applicable to predict fatigue life of 17-4 PH workpiece produced by SLM, whether transmission or bracket load histories developed by the Society of Automotive Engineers.

    摘要 I ABSTRACT II 誌謝 III 目錄 IV 圖目錄 VII 表目錄 XI 符號說明 XII 第一章 緒論 1 1.1 研究動機與目的 1 1.2 文獻回顧 6 1.2.1 積層製造析出硬化型不鏽鋼之微結構 6 1.2.2 積層製造析出硬化型不鏽鋼之機械性質 6 1.2.3 傳統製造 17-4 PH 工件之疲勞性質 7 1.2.4 積層製造 17-4 PH 工件之高週疲勞 7 第二章 理論說明 9 2.1 應力-壽命曲線 10 2.2 高週疲勞分析法 (應力-壽命法) 11 2.3 平均應力的影響 13 2.4 循環計數法 15 2.5 疲勞損傷累積 17 2.6 變動負荷振幅歷程 18 2.7 訊號壓縮 19 2.8 循序疲勞分析法 21 第三章 研究方法 23 3.1 研究流程 23 3.2 實驗試件製備 24 3.2.1 17-4 PH 不鏽鋼粉末 24 3.2.2 選擇性雷射熔融積層製造 25 3.2.3 熱處理 29 3.3 密度量測 31 3.4 硬度量測 32 3.5 表面粗糙度量測 33 3.6 拉伸實驗 34 3.7 固定負荷振幅疲勞實驗 35 3.8 變動負荷振幅疲勞實驗 36 3.9 金相、孔洞率與破斷面觀察 37 第四章 結果與討論 40 4.1 積層製造製程參數探討 40 4.1.1 密度、硬度及表面粗糙度 40 4.1.2 列印能量密度與密度、硬度及表面粗糙度之關係 42 4.1.3 較佳製程參數選擇 45 4.2 金相及孔洞觀察 48 4.2.1 金相位置標示方法 48 4.2.2 不同雷射功率的試件 49 4.2.3 不同掃描速率的試件 54 4.2.4 不同掃描間距的試件 57 4.2.5 不同列印能量密度的試件 60 4.2.6 不同密度的試件 63 4.2.7 不同硬度的試件 65 4.2.8 不同表面粗糙度的試件 67 4.2.9 有無熱處理的試件 69 4.3 拉伸性質 70 4.4 固定振幅高週疲勞性質 73 4.4.1 應力-壽命線 73 4.4.2 平均應力-應力振幅圖 (Haigh Diagram) 79 4.5 變動振幅高週疲勞性質及壽命預測 81 4.5.1 傳動軸 (TRN) 負荷歷程 82 4.5.2 支架 (BRK) 負荷歷程 84 4.6 破斷面觀察 86 4.6.1 拉伸試件 86 4.6.2 固定振幅疲勞試件 (R = -1) 89 4.6.3 變動振幅 TRN 歷程疲勞試件 91 4.6.4 變動振幅 BRK 歷程疲勞試件 93 第五章 結論 95 第六章 未來研究方向 97 參考文獻 98

    [1] D. Gu, W. Meiners, Y.-C. Hagedorn, K. Wissenbach, and R. Poprawe, "Bulk-form TiCx / Ti nanocomposites with controlled nanostructure prepared by a new method: selective laser melting," Journal of Physics D: Applied Physics, Vol. 43, No. 29, Article No. 295402, 2010.
    [2] J.-P. Kruth, M.-C. Leu, and T. Nakagawa, "Progress in additive manufacturing and rapid prototyping," Cirp Annals, Vol. 47, No. 2, pp. 525-540, 1998.
    [3] L. Thijs, F. Verhaeghe, T. Craeghs, J. Van Humbeeck, and J.-P. Kruth, "A study of the microstructural evolution during selective laser melting of Ti–6Al–4V," Acta Materialia, Vol. 58, No. 9, pp. 3303-3312, 2010.
    [4] A. Gebhardt, 3D列印導論. 全華圖書, 2017.
    [5] Y. Li, H. Yang, X. Lin, W. Huang, J. Li, and Y. Zhou, "The influences of processing parameters on forming characterizations during laser rapid forming," Materials Science and Engineering: A, Vol. 360, No. 1-2, pp. 18-25, 2003.
    [6] Z. Yu et al., "Effect of laser remelting processing on microstructure and mechanical properties of 17-4 PH stainless steel during laser direct metal deposition," Journal of Materials Processing Technology, Vol. 284, Article No. 116738, 2020.
    [7] J. Gunasekaran, P. Sevvel, and I. John Solomon, "Metallic materials fabrication by selective laser melting: A review," Materials Today: Proceedings, Vol. 37, pp. 252-256, 2021/01/01/ 2021, Doi: https://doi.org/10.1016/j.matpr.2020.05.162.
    [8] METAL AM, "Analysis of Additive Manufacturing materials from Wohlers and Senvol Database," presented at the https://www.metal-am.com/analysis-of-additive-manufacturing-materials-from-wohlers-and-senVol-database/, 2020.
    [9] J. Yao, L. Wang, Q. Zhang, F. Kong, C. Lou, and Z. Chen, "Surface laser alloying of 17-4 PH stainless steel steam turbine blades," Optics & Laser Technology, Vol. 40, No. 6, pp. 838-843, 2008, Doi: https://doi.org/10.1016/j.optlastec.2007.11.008.
    [10] 黃俊仁,“金屬疲勞課程講義第三章“,國立中央大學機械工程學系,2020。
    [11] M. B. Balajaddeh and H. Naffakh-Moosavy, "Pulsed Nd: YAG laser welding of 17-4 PH stainless steel: Microstructure, mechanical properties, and weldability investigation," Optics & Laser Technology, Vol. 119, Article No. 105651, 2019.
    [12] S. Cheruvathur, E. A. Lass, and C. E. Campbell, "Additive manufacturing of 17-4 PH stainless steel: post-processing heat treatment to achieve uniform reproducible microstructure," JOM, Vol. 68, No. 3, pp. 930-942, 2016.
    [13] A. Yadollahi and N. Shamsaei, "Additive manufacturing of fatigue resistant materials: Challenges and opportunities," International Journal of Fatigue, Vol. 98, pp. 14-31, 2017.
    [14] G. Schaffer, Aluminum Powder Metallurgy: Process, Properties and Design Solutions. Aluminum Association, 2000.
    [15] S. Kalpakjian and S. R. Schmid, Manufacturing Engineering and Technology. Pearson, 2014.
    [16] T. Furumoto et al., "Permeability and strength of a porous metal structure fabricated by additive manufacturing," Journal of Materials Processing Technology, Vol. 219, pp. 10-16, 2015.
    [17] P. Blackwell, "The mechanical and microstructural characteristics of laser-deposited IN718," Journal of materials processing technology, Vol. 170, No. 1-2, pp. 240-246, 2005.
    [18] T.-H. Hsu et al., "Microstructure and property of a selective laser melting process induced oxide dispersion strengthened 17-4 PH stainless steel," Journal of Alloys and Compounds, Vol. 803, pp. 30-41, 2019.
    [19] P. Mercelis and J. P. Kruth, "Residual stresses in selective laser sintering and selective laser melting," Rapid Prototyping Journal, Vol. 12 No. 5, pp. 254-265, https://doi.org/10.1108/13552540610707013, 2006.
    [20] D. Gu and W. Meiners, "Microstructure characteristics and formation mechanisms of in situ WC cemented carbide based hard metals prepared by selective laser melting," Materials Science and Engineering: A, Vol. 527, No. 29-30, pp. 7585-7592, 2010.
    [21] J.-H. Wu and C.-K. Lin, "Tensile and fatigue properties of 17-4 PH stainless steel at high temperatures," Metallurgical and materials transactions A, Vol. 33, No. 6, pp. 1715-1724, 2002.
    [22] B. M. Schönbauer, M. Fitzka, U. Karr, and H. Mayer, "Variable amplitude very high cycle fatigue of 17-4PH steel with a stepwise S-N curve," International Journal of Fatigue, Vol. 142, Article No. 105963, 2021.
    [23] B. M. Schönbauer, K. Yanase, and M. Endo, "VHCF properties and fatigue limit prediction of precipitation hardened 17-4 PH stainless steel," International Journal of Fatigue, Vol. 88, pp. 205-216, 2016.
    [24] D. Gu et al., "Densification behavior, microstructure evolution, and wear performance of selective laser melting processed commercially pure titanium," Acta Materialia, Vol. 60, No. 9, pp. 3849-3860, 2012.
    [25] S. Romano, P. Nezhadfar, N. Shamsaei, M. Seifi, and S. Beretta, "High cycle fatigue behavior and life prediction for additively manufactured 17-4 PH stainless steel: Effect of sub-surface porosity and surface roughness," Theoretical and Applied Fracture Mechanics, Vol. 106, Article No. 102477, 2020.
    [26] L. Carneiro, B. Jalalahmadi, A. Ashtekar, and Y. Jiang, "Cyclic deformation and fatigue behavior of additively manufactured 17-4 PH stainless steel," International Journal of Fatigue, Vol. 123, pp. 22-30, 2019.
    [27] F. Concli, L. Fraccaroli, F. Nalli, and L. Cortese, "High and low-cycle-fatigue properties of 17–4 PH manufactured via selective laser melting in as-built, machined and hipped conditions," Progress in Additive Manufacturing, pp. 1-11, 2021.
    [28] P. Nezhadfar, R. Shrestha, N. Phan, and N. Shamsaei, "Fatigue behavior of additively manufactured 17-4 PH stainless steel: Synergistic effects of surface roughness and heat treatment," International Journal of Fatigue, Vol. 124, pp. 188-204, 2019.
    [29] R. Molaei and A. Fatemi, "Fatigue performance of additive manufactured metals under variable amplitude service loading conditions including multiaxial stresses and notch effects: Experiments and modelling," International Journal of Fatigue, Vol. 145, Article No. 106002, 2021.
    [30] A. Yadollahi, N. Shamsaei, S. M. Thompson, A. Elwany, L. Bian, "Effects of building orientation and heat treatment on fatigue behavior of selective laser melted 17-4 PH stainless steel", International Journal of Fatigue, Vol. 94, Part 2, pp. 218-235, 2017.
    [31] A. Yadollahi, N. Shamsaei, S. M. Thompson, A. Elwany, L. Bian, M. Mahmoudi, "Fatigue behavior of selective laser melted 17-4 PH stainless steel", In 2015 International Solid Freeform Fabrication Symposium. University of Texas at Austin., 2015.
    [32] W. Schneller, M. Leitner, S. Leuders, J. M. Sprauel, F. Grün, T. Pfeifer, O. Jantschner, "Fatigue strength estimation methodology of additively manufactured metallic bulk material", Additive Manufacturing, Vol. 39, Article No. 101688, 2021.
    [33] J. A. Bannantine, J. J. Comer, and J. L. Hardrock, “Fundamentals of Metal Fatigue Analysis,” Prentice Hall, New Jersey, 1990.
    [34] 黃嘉彥,“工程結構之疲勞與破壞”,徐氏基金會,1998。
    [35] R. I. Stephens, A. Fatemi, R. R. Stephens, and H. O. Fuchs, “Metal Fatigue in Engineering,” John Wiley & Sons, New York, 2nd ed, 2000.
    [36] “Section 3: Metals Test Methods and Analytical Procedure, Vol. 03.01, Metals-Mechanical Testing; Elevated and Low-Temperature Tests,” American Society for Testing and Materials, United States of America, 1986.
    [37] A. Wöhler, “Ueber die Festigkeits-versuche mit Eisen und Stahl,” 1871.
    [38] 許育銓,“SA533B1 壓力槽鋼材之高週疲勞壽限評估模式研究“,國立中央大學機械工程學系所,碩士論文,2001。
    [39] 陳裕城,“機械零組件之加速耐久分析",國立中央大學,碩士論文,1991。
    [40] 網路資料:山陽特殊製鋼株式会社。取自https://www.sanyo-steel.co.jp/
    [41] 網路資料:友晁能源材料股份有限公司。取自http://www.tsemcorp.com/index.html
    [42] ASTM E564-19a, "Standard Specification for Hot-Rolled and Cold-Finished Age-Hardening Stainless Steel Bars and Shapes", ASTM International, West Conshohocken, PA (2019) www.astm.org
    [43] J. A. Slotwinski, E. J. Garboczi and K. M. Hebenstreit, "Porosity measurements and analysis for metal additive manufacturing process control," Journal of Research of the National Institute of Standards and Technology, Vol. 119, pp. 494-528, 2014.
    [44] ASTM E18-22, " Standard Test Methods for Rockwell Hardness of Metallic Materials", ASTM International, West Conshohocken, PA (2022) www.astm.org
    [45] "Surface roughness "JIS B 0601,2001.
    [46] ASTM E8-21, " Standard Test Methods for Tension Testing of Metallic Materials", ASTM International, West Conshohocken, PA (2021) www.astm.org
    [47] ASTM E466-21, " Standard Practice for Conducting Force Controlled Constant Amplitude Axial Fatigue Tests of Metallic Materials", ASTM International, West Conshohocken, PA (2021) www.astm.org
    [48] ASTM E3-11, " Standard Guide for Preparation of Metallographic Specimens", ASTM International, West Conshohocken, PA (2011) www.astm.org
    [49] M. Scurria, B. Möller, R. Wagener, & T. Bein, "Effects of different heat treatments on the cyclic material behavior of additively manufactured Inconel® 718", Procedia Structural Integrity, Vol. 18, pp. 586-593, 2019.
    [50] C.R. Rice, J.L. Jackson, J. Bakuckas, S. Thompson, Metallic Materials Properties Development and Standardization (MMPDS): Chapters 1-4. Vol. 1. National Technical Information Service, 2003.

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