跳到主要內容

簡易檢索 / 詳目顯示

研究生: 劉哲銘
C-M Liu
論文名稱: 以熱交換器法生長氧化鋁單晶與晶體檢測
指導教授: 陳志臣
Jyh-Chen Chen
口試委員:
學位類別: 碩士
Master
系所名稱: 工學院 - 機械工程學系
Department of Mechanical Engineering
畢業學年度: 88
語文別: 中文
論文頁數: 62
中文關鍵詞: 熱交換器法氧化鋁晶體
外文關鍵詞: HEM, Sapphire, Crystal
相關次數: 點閱:13下載:0
分享至:
查詢本校圖書館目錄 查詢臺灣博碩士論文知識加值系統 勘誤回報

  • 本研究也針對利用熱交換器法所生長出之Sapphire晶體作一系列的檢測,例如利用穿透式及反射式光學顯微鏡(Optical-Microscope)及掃描式電子顯微鏡(Scanning-Electron-Microscope)觀察晶體之微觀組織,比較在不同的生長條件下其結構組織之不同,並與品質良好之氧化鋁單晶做比較,同時探討晶體中缺陷產生之原因,另外還利用能譜儀(Energy-Dispersive-Spectrometer)來對晶體之成分做分析,以確定污染物之種類及分佈狀況,且為了要了解晶體缺陷對晶體硬度之影響,還利用微硬度測試儀來測試所生長出之晶體硬度,比較與單晶的差異,希望能藉這些檢測來作為改善晶體品質之依據,以期能生長出高品質、高純度之晶體。


    摘要..................................................I 致謝..................................................II 目錄..................................................III 圖表目錄..............................................V 第一章 序論...........................................1 1.1熱交換器法之簡介.................................1 1.2氧化鋁晶體性質與應用..........................2 1.3 文獻回顧..........................................3 1.4 研究動機..........................................5 第二章晶體生長........................................6 2.1實驗設備...........................................6 2.2實驗...............................................8 2.2.1實驗前之準備工作...............................8 2.2.2實驗步驟.........................................9 2.2.3長晶過程及現象之探討.......................10 2.3 長晶結果..........................................12 2.3.1 利用降溫來生長晶體..........................13 2.3.2 利用增加氦氣流量生長晶體.............15 2.4 結論............................................................16 第三章 晶體之檢測及缺陷之研究............17 3.1 缺陷之種類........................................17 3.2檢測之方法.........................................17 3.3缺陷分析...........................................18 3.3.1氣孔分析.........................................18 3.3.2 樹枝狀結構分析..................................19 3.3.3 差排分析........................................20 3.4晶種之檢測.........................................20 3.5晶體之檢測.........................................21 3.6結論...............................................23 第四章 總結論.........................................24 4.1 結論..............................................24 4.2 未來方向..........................................24 參考文獻..............................................58

    [1] D. Viechnicki and F. Schmid , “ Growth of sapphire disk from the melt by a gradient furnace technique ”, Journal of the American Ceramic Society-Discussions and Notes 53:9(1970)528
    [2] F. Schmid and D. J. Viechnicki , “Apparatus and method for undirectionally solidifying high temperature material” , U.S. Patent 3,653,432 (1972)
    [3] D. Viechnicki and F. Schmid , “ Crystal growth using the heat exchanger method (HEM) ” , Journal of Crystal Growth 26 (1974) 162
    [4] F. Schmid, “ Crystal Growing “ , U.S. Patent 3,898,051 (1975)
    [4] F. Schmid, “ Crystal Growing “ , U.S. Patent 3,898,051 (1975)
    [6] J. L. Caslavsky and D. Viechnicki , “ Melt growth of Nd:Y3Al5O12(Nd:YAG) using the heat exchanger method (HEM) “ , Journal of Crystal Growth 46 (1979) 601
    [7] F. Schmid and D. J. Viechnicki , “Crystal Growing “ , U.S. Pat. 4,256,530 (1981)
    [8] F. Schmid , C. P. Khattak and M.B. Smith , “ Growth of Bismuth Germanate crystal by the Heat Exchanger Method “ , Journal of Crystal Growth 70 (1984) 466
    [8] F. Schmid , C. P. Khattak and M.B. Smith , “ Growth of Bismuth Germanate crystal by the Heat Exchanger Method “ , Journal of Crystal Growth 70 (1984) 466
    [10] F. Schmid and C.P. Khattak , “ Growth of near-net-shaped sapphire domes using the heat exchanger method ” , Materials Letters 7: 9,10 (1989)318
    [11] 紀俊安, “HEM長晶系統之設計 “ , 國立中央大學碩士論文(1999)
    [12] 余樹楨 , “ 晶體之結構與性質 ” , 渤海堂文化公司 (1987)
    [12] 余樹楨 , “ 晶體之結構與性質 ” , 渤海堂文化公司 (1987)
    [14] S.Nakamura , T.Mukai and M.Senoh , “ Candela-class high-brightness InGaN/AlGaN double-heterostructure blue-light-emitting diodes” , Applied Physsics Letters 64 (1994) 1687
    [14] S.Nakamura , T.Mukai and M.Senoh , “ Candela-class high-brightness InGaN/AlGaN double-heterostructure blue-light-emitting diodes” , Applied Physsics Letters 64 (1994) 1687
    [16] J. L. Caslavsky , “The growth of large diameter single crystals by vertical solidification of the melt “ , Crystal Growth of Electronic Materials(1985)113
    [16] J. L. Caslavsky , “The growth of large diameter single crystals by vertical solidification of the melt “ , Crystal Growth of Electronic Materials(1985)113
    [16] J. L. Caslavsky , “The growth of large diameter single crystals by vertical solidification of the melt “ , Crystal Growth of Electronic Materials(1985)113
    [16] J. L. Caslavsky , “The growth of large diameter single crystals by vertical solidification of the melt “ , Crystal Growth of Electronic Materials(1985)113
    [20] F. Theodore , T. Duffar and F. Louchet , “Modelling plastic stress relaxation in shaped sapphire crystal growth ” , Journal of Crystal Growth 198/199 (1999) 232
    [20] F. Theodore , T. Duffar and F. Louchet , “Modelling plastic stress relaxation in shaped sapphire crystal growth ” , Journal of Crystal Growth 198/199 (1999) 232
    [22] F. Schmid , C. P. Khattak and D. Mark Felt , “ Producing large sapphire for optic applications ” , Journal American Ceramic Society Bullet 73:2 (1994) 39
    [23] F. Schmid and D. C. Harris , “ Effects of crystal orientation and temperature on the strength of sapphire ” , Journal American Ceramic Society 81 (1998) 885
    [24] J. A. Savage , “ Reparation and properties of hard crystalline materials for optical applications” , Journal of Crystal Growth 113 (1991) 698
    [25] D. C. Harris , “ Infrared window and dome materials ” , SPIE Optical Engineering Press(1992)
    [26] Chen et al , “ Method of making thermal shock resistant sapphire for IR Windows and Domes ” , U.S. Patent. 5,702,654 (1997)
    [27] A.Horowitz , S. Biderman , Y. Einav, G. Ben Amar, D. Gazit, “ Improved control of sapphire crystal growth ” , Journal of Crystal Growth 167 (1996) 183
    [28] C. W. Lu , J. C. Chen , “ Numerieal coputation of the sapphire crystal growth using heat exchanger method ” , 投稿中
    [29] 劉偉隆 , 林淳杰 , 曾春風 , 陳文照 , “ 物理冶金 ” , 全華科技圖書(1996)
    [30] D. Viechnicki and F. Schmid , “ Growth of large monocrystal of Al2O3 by a gradient furnace technique ” , Journal of Crystal Growth 11(1971)345
    [31] F. Schmid and C. P. Khattak , “Large crystal sapphire optics “ , Laser Focus/Electro-Optics Sep. (1983) 147
    [32] C. P. Khattak and F. Schmid , “ Growth of large-diameter by HEMTM for optical and laser application “ , SPIE Advance in Optical Materials 505 (1984) 4
    [33] C.P.Khattak and A. N. Scoville , “ Growth of laser crystals by heat exchanger method (HEM) ” , SPIE Laser and Nonlinear Optical Materials 68 (1986) 58
    [33] C.P.Khattak and A. N. Scoville , “ Growth of laser crystals by heat exchanger method (HEM) ” , SPIE Laser and Nonlinear Optical Materials 68 (1986) 58
    [35] F. Schmid and C. P. Khattak , “ Current status of sapphire technology for window and dome applications “ , SPIE Window and Dome Technologies and Materials1112 (1989) 25
    [36] C. P. Khattak and F. Schmid , “ Growth of CdTe crystal by the heat exchanger method (HEMTM) ”, SPIE Future Infrared Detector Materials 1106 (1989)47
    [36] C. P. Khattak and F. Schmid , “ Growth of CdTe crystal by the heat exchanger method (HEMTM) ”, SPIE Future Infrared Detector Materials 1106 (1989)47
    [38] F. Schmid , M. B. Smith and C. P. Khattak , “Current status of sapphire dome production ” , SPIE 2286(1994)2
    [39] C. P. Khattak , F. Schmid , “High-Efficiency solar cells using HEM silicon ” , IEEE (1994) 1351
    [39] C. P. Khattak , F. Schmid , “High-Efficiency solar cells using HEM silicon ” , IEEE (1994) 1351
    [41] C. P. Khattak and F. Schmid , “ Automation in HEM silicon ingot production ” , IEEE (1996) 597
    [42] C. P. Khattak and F. Schmid , “ Growth and characterization of 200 kg multicrysalline silicon ingots by HEM ” , IEEE (1997) 111
    [43] J. H. Wang , D. H. Kim , J. S. Huh , “ Modeling of crystal growth process in heat exchanger method ” , Journal of Crystal Growth 174 (1997) 13
    [44] Y. Z. Zhou , “ Growth of high quality large Nd:YAG crystals by temperature gradient technique ” , Journal of Crystal Growth 78 (1986) 31
    [44] Y. Z. Zhou , “ Growth of high quality large Nd:YAG crystals by temperature gradient technique ” , Journal of Crystal Growth 78 (1986) 31
    [44] Y. Z. Zhou , “ Growth of high quality large Nd:YAG crystals by temperature gradient technique ” , Journal of Crystal Growth 78 (1986) 31
    [44] Y. Z. Zhou , “ Growth of high quality large Nd:YAG crystals by temperature gradient technique ” , Journal of Crystal Growth 78 (1986) 31
    [44] Y. Z. Zhou , “ Growth of high quality large Nd:YAG crystals by temperature gradient technique ” , Journal of Crystal Growth 78 (1986) 31

    QR CODE
    :::